[H₂BIM(tBu)BPh₂]PF₆

Base Information

• Chemical Name: [H₂BIM(tBu)BPh₂]PF₆
• CAS No.: 1160462-22-5
• Molecular Formula: C₂₆H₃₄BN₄*F₆P
• Molecular Weight: 558.358

Synonyms:

Chemical Property of [H₂BIM(tBu)BPh₂]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [H₂BIM(tBu)BPh₂]PF₆

There total 1 articles about [H₂BIM(tBu)BPh₂]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

ammonium hexafluorophosphate + [H2BIM(tBu)BPh2]Cl (1160462-16-7) → [H2BIM(tBu)BPh2]PF6 (1160462-22-5)

Guidance literature:

In methanol; to a soln. of B-contg. compd. (6.7 mmol) in MeOH was added in several portions well-milled NH4PF6 (20.1 mmol); stirring at room temp. for several hours; the solids were filtered off and washed on the filter with MeOH; the remaining solid was washed with CH2Cl2 and the filtrate was evapd.; recrystn. from CH2Cl2-MeOH; elem. anal.;

DOI:10.1021/om801097f

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + diethyl ether (60-29-7,927820-24-4) + [H2BIM(tBu)BPh2]PF6 (1160462-22-5) → [(BIM(tBu)BPh2)Li(OEt2)]

Guidance literature:

In diethyl ether; hexane; under Ar; to a suspn. of B-contg. compd. (0.54 mmol) in Et2O was added at -70°C a soln. of n-BuLi (1.096 mmol) in hexane; the mixt. was allowed to warm to ambient temp. and then was stirred for 3 h; the solvent was removed at 1E-3 mbar and the residue was extd. with abs.pentane and evapd.;

DOI:10.1021/om801097f

upstream raw materials:

[H₂BIM(tBu)BPh₂]Cl

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1160462-22-5 [H₂BIM(tBu)BPh₂]PF₆

Send

Send

Metric Ton KG G Pound L ML

Send

Send