(3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Base Information Edit

Chemical Name:(3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol
CAS No.:105079-21-8
Molecular Formula:C₂₉H₄₀N₂O₂
Molecular Weight:448.649
Hs Code.:
Mol file:105079-21-8.mol

(3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

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Chemical Property of (3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol Edit

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Technology Process of (3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

There total 3 articles about (3S,8S,9S,10R,13S,14S,17R)-17-{(R)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78873-43-5
3β-(Tetrahydropyranyloxy)-22-iodo-23,24-bisnorchol-5-ene

: 105079-21-8
(3S,8S,9S,10R,13S,14S,17R)-17-{(S)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / tetrahydrofuran; hexamethylphosphoric acid triamide

2: acid

With acid; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1248/cpb.34.931

Reference yield:

: 80863-11-2
sodium m-(3H-diazirino)phenoxide

: 105079-21-8
(3S,8S,9S,10R,13S,14S,17R)-17-{(S)-2-[3-(3H-Diazirin-3-yl)-phenoxy]-1-methyl-ethyl}-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / tetrahydrofuran; hexamethylphosphoric acid triamide

2: acid

With acid; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1248/cpb.34.931