Technology Process of C38H40N4O7S
There total 14 articles about C38H40N4O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 - 8 h / Cooling with ice
2: hydrogen bromide; acetic acid / 1.5 h / 20 °C
3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / Cooling with ice
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: palladium 10% on activated carbon / 40 °C
2.1: 4-methyl-morpholine / acetonitrile / Cooling with ice
3.1: dichloromethane / 1 h
4.1: chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C / Reflux
4.2: 20 °C / pH 8 - 9 / Cooling with ice
5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 - 8 h / Cooling with ice
6.1: hydrogen bromide; acetic acid / 1.5 h / 20 °C
7.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / Cooling with ice
With
4-methyl-morpholine; chloro-trimethyl-silane; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 7 steps
1: palladium 10% on activated carbon / 40 °C
2: 4-methyl-morpholine / acetonitrile / Cooling with ice
3: ethanol
4: dichloromethane / 1 h
5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 - 8 h / Cooling with ice
6: hydrogen bromide; acetic acid / 1.5 h / 20 °C
7: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / Cooling with ice
With
4-methyl-morpholine; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm2011996