2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine

Base Information

• Chemical Name: 2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine
• CAS No.: 36961-29-2
• Molecular Formula: C₁₆H₁₅N₃
• Molecular Weight: 249.315
• Mol file: 36961-29-2.mol

Synonyms:

Chemical Property of 2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine

There total 1 articles about 2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.5%

benzamidine monohydrochloride (1670-14-0) + acetaldehyde (75-07-0,9002-91-9) → 2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine (36961-29-2)

Guidance literature:

benzamidine monohydrochloride; With sodium hydroxide; In dichloromethane; water; for 0.166667h;

acetaldehyde; In dichloromethane; at 20 ℃; for 19h;

DOI:10.1002/chem.201100433

Reference yield: 63.0%

2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine (36961-29-2) → 2-methyl-4,6-diphenyl-1,3,5-triazine (3599-62-0) + 2-methyl-4,6-diphenyl-1,3,5-triazine-1-oxide (1345690-23-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; Reflux;

DOI:10.1002/chem.201100433

Reference yield:

2-methyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine (36961-29-2) → 2,2-dimethyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine-1-oxide (1345690-24-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / Reflux

2: diethyl ether

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; chloroform;

DOI:10.1002/chem.201100433

upstream raw materials:

benzamidine monohydrochloride

acetaldehyde

Downstream raw materials:

2-methyl-4,6-diphenyl-1,3,5-triazine

2-methyl-4,6-diphenyl-1,3,5-triazine-1-oxide

2,2-dimethyl-4,6-diphenyl-1,2-dihydro-1,3,5-triazine-1-oxide

2,2-dimethyl-2,4-diphenyl-1,2-dihydro-1,3,5-triazinyl-1-oxy

Refernces