C₁₅H₁₉NO₂S

Base Information

Chemical Name:C₁₅H₁₉NO₂S
CAS No.:1374550-66-9
Molecular Formula:C₁₅H₁₉NO₂S
Molecular Weight:277.387
Hs Code.:

C<sub>15</sub>H<sub>19</sub>NO<sub>2</sub>S

Synonyms:

Suppliers and Price of C₁₅H₁₉NO₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₉NO₂S

Chemical Property:

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Technology Process of C₁₅H₁₉NO₂S

There total 9 articles about C₁₅H₁₉NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374550-62-5
C₁₆H₁₈F₃NO₅S₂

: 1374550-66-9
C₁₅H₁₉NO₂S

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine; In N,N-dimethyl-formamide; at 80 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1002/asia.201101029

Reference yield:

: 1374550-49-8
N-(4-(1-hydroxycyclobutyl)but-3-yn-1-yl)-4-methylbenzenesulfonamide

: 1374550-66-9
C₁₅H₁₉NO₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); toluene-4-sulfonic acid / dichloromethane / 4 h / 25 °C / Molecular sieve; Darkness

2.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.58 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 0.67 h / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine; trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; ethylbenzene; N,N-dimethyl-formamide;
DOI:10.1002/asia.201101029

Reference yield:

: 1374550-81-8
C₁₅H₁₉NO₃S

: 1374550-66-9
C₁₅H₁₉NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.58 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 0.67 h / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine; lithium hexamethyldisilazane; In tetrahydrofuran; ethylbenzene; N,N-dimethyl-formamide;
DOI:10.1002/asia.201101029