C₅₇H₆₈Cl₃N₃O₇S₂Si

Base Information

Chemical Name:C₅₇H₆₈Cl₃N₃O₇S₂Si
CAS No.:1374451-22-5
Molecular Formula:C₅₇H₆₈Cl₃N₃O₇S₂Si
Molecular Weight:1105.76
Hs Code.:

C<sub>57</sub>H<sub>68</sub>Cl<sub>3</sub>N<sub>3</sub>O<sub>7</sub>S<sub>2</sub>Si

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Chemical Property of C₅₇H₆₈Cl₃N₃O₇S₂Si

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Technology Process of C₅₇H₆₈Cl₃N₃O₇S₂Si

There total 6 articles about C₅₇H₆₈Cl₃N₃O₇S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374451-20-3
C₃₆H₄₃Cl₃N₂O₆S

: 1374451-22-5
C₅₇H₆₈Cl₃N₃O₇S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

2: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; boron trifluoride diethyl etherate; t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1055/s-0031-1290339

Reference yield:

: C₃₁H₃₅Cl₃N₂O₄S

: 1374451-22-5
C₅₇H₆₈Cl₃N₃O₇S₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1055/s-0031-1290339

Reference yield:

: C₈H₁₇NO₃

: 1374451-22-5
C₅₇H₆₈Cl₃N₃O₇S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2: sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

4: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

5: (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

6: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; (7-azabenzotriazol-1-yl)-oxy-tris(pyrrolidino)phosphonium hexafluorophosphate; boron trifluoride diethyl etherate; t-butyldimethylsiyl triflate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1055/s-0031-1290339