C₃₄H₄₅NO₇Si

Base Information

Chemical Name:C₃₄H₄₅NO₇Si
CAS No.:1408236-89-4
Molecular Formula:C₃₄H₄₅NO₇Si
Molecular Weight:607.819
Hs Code.:

C<sub>34</sub>H<sub>45</sub>NO<sub>7</sub>Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₅NO₇Si

Chemical Property:

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Technology Process of C₃₄H₄₅NO₇Si

There total 9 articles about C₃₄H₄₅NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3377-21-7
dimethyl 2-methylenemalonate

: C₂₈H₃₇NO₃Si

: 1408236-89-4
C₃₄H₄₅NO₇Si

Guidance literature:: In dichloromethane; at 20 ℃; for 60h; diastereoselective reaction;
DOI:10.1021/ol3027945

Reference yield:

: 133-13-1
ethyl diethyl malonate

: 1408236-89-4
C₃₄H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydride / diethyl ether / Reflux

2: potassium hydroxide / water; ethanol / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

4: manganese(IV) oxide / dichloromethane / 20 °C

5: dichloromethane / 3 h / 20 °C

6: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C

7: 1H-imidazole / dichloromethane / 1.5 h / 0 - 20 °C

8: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 18 h / 100 °C

9: dichloromethane / 60 h / 20 °C

With 1H-imidazole; manganese(IV) oxide; copper(l) iodide; lithium aluminium tetrahydride; sodium hydride; diisobutylaluminium hydride; caesium carbonate; potassium hydroxide; N,N`-dimethylethylenediamine; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; 5: |Wittig Olefination / 9: |Diels-Alder Cycloaddition;
DOI:10.1021/ol3027945

Reference yield:

: C₅H₉IO

: 1408236-89-4
C₃₄H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 6 steps

1: manganese(IV) oxide / dichloromethane / 20 °C

2: dichloromethane / 3 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C

4: 1H-imidazole / dichloromethane / 1.5 h / 0 - 20 °C

5: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 18 h / 100 °C

6: dichloromethane / 60 h / 20 °C

With 1H-imidazole; manganese(IV) oxide; copper(l) iodide; diisobutylaluminium hydride; caesium carbonate; N,N`-dimethylethylenediamine; In hexane; dichloromethane; N,N-dimethyl-formamide; 2: |Wittig Olefination / 6: |Diels-Alder Cycloaddition;
DOI:10.1021/ol3027945