C₃₀H₃₃N₃O

Base Information

Chemical Name:C₃₀H₃₃N₃O
CAS No.:1340580-72-4
Molecular Formula:C₃₀H₃₃N₃O
Molecular Weight:451.612
Hs Code.:

C<sub>30</sub>H<sub>33</sub>N<sub>3</sub>O

Synonyms:

Suppliers and Price of C₃₀H₃₃N₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₃N₃O

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₀H₃₃N₃O

There total 7 articles about C₃₀H₃₃N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1340580-72-4
C₃₀H₃₃N₃O

Guidance literature:: Multi-step reaction with 8 steps

1: N-Bromosuccinimide; ammonium acetate / diethyl ether / 0.5 h / 20 °C

2: 2-methoxy-ethanol / 12 h / 130 °C / Inert atmosphere

3: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

5: triethylamine / dichloromethane / 2 h / 0 - 20 °C

6: lithium hydroxide / tetrahydrofuran; methanol; water / 24 h / 50 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

8: hydrogenchloride / ethyl acetate

With hydrogenchloride; dmap; N-Bromosuccinimide; ammonium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 2-methoxy-ethanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e

Reference yield:

: 21660-16-2
1,2,3,4-tetrahydrocarbazole-6-carboxylic acid ethyl ester

: 1340580-72-4
C₃₀H₃₃N₃O

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

3: triethylamine / dichloromethane / 2 h / 0 - 20 °C

4: lithium hydroxide / tetrahydrofuran; methanol; water / 24 h / 50 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

6: hydrogenchloride / ethyl acetate

With hydrogenchloride; dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e

Reference yield:

: 1340581-01-2
ethyl 9-(3-bromopropyl)-2,3,4,9-tetrahydro-1H-carbazole-6-carboxylate

: 1340580-72-4
C₃₀H₃₃N₃O

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

3: lithium hydroxide / tetrahydrofuran; methanol; water / 24 h / 50 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 20 °C

5: hydrogenchloride / ethyl acetate

With hydrogenchloride; dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e