13-cis-9-demethylretinal

Base Information

Chemical Name:13-cis-9-demethylretinal
CAS No.:52152-30-4
Molecular Formula:C₁₉H₂₆O
Molecular Weight:270.415
Hs Code.:

Synonyms:

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Chemical Property of 13-cis-9-demethylretinal

Chemical Property:

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Technology Process of 13-cis-9-demethylretinal

There total 9 articles about 13-cis-9-demethylretinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14393-45-4
(E)-3-(2,6,6-trimethylcyclohex-1-enyl)acrylic acid

: 52152-30-4
13-cis-9-demethylretinal

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / LiAlH₄ / tetrahydrofuran / 1a) 0 deg C to room temperature, 30 min, 1b) room temperature, 1 h

2: 82 percent / activated MnO₂ / petroleum ether / 6 h

3: 1.) sodium hydride / 1.) THF, 0-20 deg C, 2.) ice-bath temperature to room temperature

4: 90 percent / diisobutylaluminium hydride

5: 1.) sodium hydride / 1.) THF, 0 deg C to room temperature, 30 min, 2.) 0 deg C to room temperature, 60 min

6: diisobutylaluminium hydride

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; Petroleum ether;

Reference yield:

: 14393-44-3
(E)-3-(2,6,6-trimethylcyclohex-1-en-1-yl)prop-2-en-1-ol

: 52152-30-4
13-cis-9-demethylretinal

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / activated MnO₂ / petroleum ether / 6 h

2: 1.) sodium hydride / 1.) THF, 0-20 deg C, 2.) ice-bath temperature to room temperature

3: 90 percent / diisobutylaluminium hydride

4: 1.) sodium hydride / 1.) THF, 0 deg C to room temperature, 30 min, 2.) 0 deg C to room temperature, 60 min

5: diisobutylaluminium hydride

With manganese(IV) oxide; sodium hydride; diisobutylaluminium hydride; In Petroleum ether;

Reference yield:

: 53018-97-6,4951-40-0
(E)-3-(2,6,6-Trimethyl-cyclohex-1-enyl)-propenal

: 52152-30-4
13-cis-9-demethylretinal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) THF, 0-20 deg C, 2.) ice-bath temperature to room temperature

2: 90 percent / diisobutylaluminium hydride

3: 1.) sodium hydride / 1.) THF, 0 deg C to room temperature, 30 min, 2.) 0 deg C to room temperature, 60 min

4: diisobutylaluminium hydride

With sodium hydride; diisobutylaluminium hydride;