αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

Base Information

Chemical Name:αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester
CAS No.:15028-49-6
Molecular Formula:C₂₆H₃₃N₃O₆
Molecular Weight:483.565
Hs Code.:

Synonyms:

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Chemical Property of αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

Chemical Property:

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Technology Process of αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

There total 5 articles about αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15030-72-5
Z-Aib-OH

: 15028-49-6
αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: Py

2: Et₃N, imidazole / dimethylformamide

3: N₂H₄*H₂O / methanol

4: (i) HCl, nBuONO, THF, (ii) /BRN= 3911480/, Et₃N, AcOEt

With pyridine; 1H-imidazole; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(67)80036-X

Reference yield:

: 15030-75-8
Z-Aib-ONp

: 15028-49-6
αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, imidazole / dimethylformamide

2: N₂H₄*H₂O / methanol

3: (i) HCl, nBuONO, THF, (ii) /BRN= 3911480/, Et₃N, AcOEt

With 1H-imidazole; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(67)80036-X

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 15028-49-6
αand-Benzyloxycarbonylamino-isobutyryl-DL-Phe-α-aminoisobuttersaeure-methylester

Guidance literature:: Multi-step reaction with 5 steps

1: OH^- / acetone

2: Py

3: Et₃N, imidazole / dimethylformamide

4: N₂H₄*H₂O / methanol

5: (i) HCl, nBuONO, THF, (ii) /BRN= 3911480/, Et₃N, AcOEt

With pyridine; 1H-imidazole; hydroxide; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4020(67)80036-X