tris(cyclohexyl)tin isothiocyanate

Base Information

Chemical Name:tris(cyclohexyl)tin isothiocyanate
CAS No.:31710-09-5
Molecular Formula:C₁₉H₃₃NSSn
Molecular Weight:426.254
Hs Code.:

Synonyms:

Suppliers and Price of tris(cyclohexyl)tin isothiocyanate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of tris(cyclohexyl)tin isothiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tris(cyclohexyl)tin isothiocyanate

There total 5 articles about tris(cyclohexyl)tin isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 17356-08-0
thiourea

: 13121-70-5
cyhexatin

: 13121-76-1
bis(tricyclohexyltin)sulfide

: 31710-09-5
tris(cyclohexyl)tin isothiocyanate

Guidance literature:: In melt; byproducts: NH3, H2O; under N2 stream, equimolar amt. of educts gradually heated to 180-200°C, then temp. retained at 130-140.degree for 4 h; crude product was refluxed in CHCl3, filtered off, filtrate concd., kept in ice cold water for 15 min, The ((C6H11)3Sn)2S filtered, elem. anal., filtrate concd., the (C6H11)3NCS recrystd. from petroleum ether;

Reference yield:

: 13121-70-5
cyhexatin

: 31710-09-5
tris(cyclohexyl)tin isothiocyanate

Guidance literature:: With NH₄NCS; In methyl cyclohexane; recrystd. from toluene; elem. anal.;

Reference yield:

: 540-72-7
sodium thiocyanide

: 3091-32-5
tricyclohexyltin(IV) chloride

: 31710-09-5
tris(cyclohexyl)tin isothiocyanate

Guidance literature:: In acetone; soln. of Sn-compound in acetone and a suspn. of NaNCS in acetone mixed; stirred at room temp. overnight; filtered; filtrate collected; filtrate shaken with a further suspn. of NaNCS in acetone for 4 h; volatiles removed by rotary evapn.; residue extracted into CHCl3; dried and rotary evapd.; recrystallized from CH2Cl2/hexane;
DOI:10.1016/j.poly.2004.08.001