Technology Process of (5S)-3-O-Benzyl-3-C-methyl-5-(9',10'-dihydro-1',4',5'-trihydroxy-9',10'-dioxo-2-anthryl)-α,β-D-ribopyranose
There total 18 articles about (5S)-3-O-Benzyl-3-C-methyl-5-(9',10'-dihydro-1',4',5'-trihydroxy-9',10'-dioxo-2-anthryl)-α,β-D-ribopyranose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 123 g / diethyl ether / 3 h / Heating
2: NaH / 1) 70 deg C, 1.5 h, 2) 70 deg C, 2 h
3: 8.6 g / 70percent aq. AcOH / 24 h / Ambient temperature
4: 8.07 g / NaIO4 / aq. acetic acid / 24 h / Ambient temperature
5: 1) DBN, 2) air / 1) DMF, o deg C, 45 min, 2) 90 min
6: 1.02 g / aq. acetic acid / 3 h / Heating
With
sodium periodate; air; 2,6-dichloro-benzonitrile; sodium hydride; acetic acid;
In
diethyl ether; acetic acid;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 123 g / diethyl ether / 3 h / Heating
2: NaH / 1) 70 deg C, 1.5 h, 2) 70 deg C, 2 h
3: 8.6 g / 70percent aq. AcOH / 24 h / Ambient temperature
4: 8.07 g / NaIO4 / aq. acetic acid / 24 h / Ambient temperature
5: 1) DBN, 2) air / 1) DMF, o deg C, 45 min, 2) 90 min
6: 1.02 g / 70percent aq. AcOH / 3 h / Ambient temperature
With
sodium periodate; air; 2,6-dichloro-benzonitrile; sodium hydride; acetic acid;
In
diethyl ether; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 8.07 g / NaIO4 / aq. acetic acid / 24 h / Ambient temperature
2: 1) DBN, 2) air / 1) DMF, o deg C, 45 min, 2) 90 min
3: 1.02 g / aq. acetic acid / 3 h / Heating
With
sodium periodate; air; 2,6-dichloro-benzonitrile;
In
acetic acid;