[Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]

Base Information

Chemical Name:[Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]
CAS No.:207917-43-9
Molecular Formula:C₂₀H₁₇ClZr
Molecular Weight:384.032
Hs Code.:

Synonyms:

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Chemical Property of [Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]

Chemical Property:

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Technology Process of [Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]

There total 2 articles about [Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 80155-52-8
(η5-cyclopentadienyl)(η5-indenyl) zirconium(IV) dichloride

: 301336-68-5
[Zr(η5-C5H5)(η5-C9H7)(C6H5)2]

: 207917-43-9
[Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]

Guidance literature:: With LiCl; In tetrahydrofuran; Ar atmosphere; addn. of THF to C14H12Cl2Zr, C26H22Zr and LiCl at room temp., mixt. stirred at 40°C in the absence of light for 15 h; solvent removed under reduced pressure, pentane added, suspn. stirred at 40°C for 1 h, filtered, concd., cooled to -18°C for 64 h, ppt.;
DOI:10.1016/S0022-328X(00)00253-9

Reference yield:

: (+)-β-chlorodiisopinocampheylborane

: 301336-68-5
[Zr(η5-C5H5)(η5-C9H7)(C6H5)2]

: 207917-43-9
[Zr(η5-C5H5)(η5-C9H7)(C6H5)Cl]

: (C₁₀H₁₇)2BC₆H₅

Guidance literature:: In toluene; to toluene soln. of C26H22Zr toluene soln. of (C10H17)2BCl was added, stirred overnight; solvent removed in vac., C20H17ClZr not isolated, detected by NMR;
DOI:10.1016/S0022-328X(00)00253-9