C₂₂H₃₀ClN₃O₇S

Base Information

Chemical Name:C₂₂H₃₀ClN₃O₇S
CAS No.:934477-05-1
Molecular Formula:C₂₂H₃₀ClN₃O₇S
Molecular Weight:516.015
Hs Code.:

C<sub>22</sub>H<sub>30</sub>ClN<sub>3</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₂₂H₃₀ClN₃O₇S

Chemical Property:

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Technology Process of C₂₂H₃₀ClN₃O₇S

There total 12 articles about C₂₂H₃₀ClN₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (5-amino-2-chloro-phenyl)-acetic acid

: 934477-05-1
C₂₂H₃₀ClN₃O₇S

Guidance literature:: Multi-step reaction with 7 steps

1: HCl

2: tetrahydrofuran / 50 °C

3: K₂CO₃; Bu₄NF / toluene

4: aq. NaOH

5: HCl

6: DIEA / CHCl₃

With hydrogenchloride; sodium hydroxide; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; toluene; 1: Fisher esterification;
DOI:10.1016/j.bmcl.2006.11.078

Reference yield:

: 409082-02-6
ethyl 2-(5-amino-2-chlorophenyl)acetate

: 934477-05-1
C₂₂H₃₀ClN₃O₇S

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 50 °C

2: K₂CO₃; Bu₄NF / toluene

3: aq. NaOH

4: HCl

5: DIEA / CHCl₃

With hydrogenchloride; sodium hydroxide; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; toluene;
DOI:10.1016/j.bmcl.2006.11.078

Reference yield:

: 200214-48-8
tert-butyl N-[4-chloro-3-(hydroxymethyl)phenyl]carbamate

: 934477-05-1
C₂₂H₃₀ClN₃O₇S

Guidance literature:: Multi-step reaction with 10 steps

1: DIEA / CH₂Cl₂

2: KI; 18-Crown-6 / ethanol

3: aq. H₂SO₄ / methanol

4: HCl

5: tetrahydrofuran / 50 °C

6: K₂CO₃; Bu₄NF / toluene

7: aq. NaOH

8: HCl

9: DIEA / CHCl₃

With hydrogenchloride; sodium hydroxide; 18-crown-6 ether; sulfuric acid; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; toluene; 4: Fisher esterification;
DOI:10.1016/j.bmcl.2006.11.078