Technology Process of C32H40IN3O3
There total 9 articles about C32H40IN3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-Bromosuccinimide / tetrahydrofuran / -40 °C
2: sodium tetrahydroborate / ethanol / -78 °C
3: potassium hydroxide / ethanol
4: isopropyl alcohol / 70 °C
5: dichloromethane / 0 °C
6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / 0 - 20 °C
With
sodium tetrahydroborate; N-Bromosuccinimide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.201102078
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 0 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / 0 - 20 °C
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane;
DOI:10.1002/chem.201102078
- Guidance literature:
-
Multi-step reaction with 7 steps
1: lithium hexamethyldisilazane / tetrahydrofuran
2: N-Bromosuccinimide / tetrahydrofuran / -40 °C
3: sodium tetrahydroborate / ethanol / -78 °C
4: potassium hydroxide / ethanol
5: isopropyl alcohol / 70 °C
6: dichloromethane / 0 °C
7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / 0 - 20 °C
With
sodium tetrahydroborate; N-Bromosuccinimide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.201102078