C₂₇H₄₈O₅Si₂

Base Information

Chemical Name:C₂₇H₄₈O₅Si₂
CAS No.:1388153-25-0
Molecular Formula:C₂₇H₄₈O₅Si₂
Molecular Weight:508.846
Hs Code.:

C<sub>27</sub>H<sub>48</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₂₇H₄₈O₅Si₂

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Technology Process of C₂₇H₄₈O₅Si₂

There total 9 articles about C₂₇H₄₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388152-91-7
C₂₁H₃₄O₅Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1388153-25-0
C₂₇H₄₈O₅Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-88-2
C₁₄H₂₀O₄

: 1388153-25-0
C₂₇H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

4: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

5: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

6: tetrahydrofuran / 0.83 h / 20 °C

7: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

8: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-89-3
C₁₄H₁₆O₄

: 1388153-25-0
C₂₇H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

3: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

4: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5: tetrahydrofuran / 0.83 h / 20 °C

6: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

7: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z