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Technology Process of trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2

trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2

Base Information
  • Chemical Name:trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2
  • CAS No.:89497-19-8
  • Molecular Formula:C35H33Cl3NiP2
  • Molecular Weight:680.644
  • Hs Code.:
trans-Ni(CClCCl<sub>2</sub>)(C<sub>6</sub>H<sub>4</sub>Me-2)(PMePh<sub>2</sub>)2

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Chemical Property of trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2
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Technology Process of trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2

There total 1 articles about trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

trans-[Ni(CClCCl<sub>2</sub>)Cl(PMePh<sub>2</sub>)2]

trans-[Ni(CClCCl2)Cl(PMePh2)2]

2-methylphenyl bromide
95-46-5

2-methylphenyl bromide

trans-Ni(CClCCl<sub>2</sub>)(C<sub>6</sub>H<sub>4</sub>Me-2)(PMePh<sub>2</sub>)2
89467-80-1,89497-19-8

trans-Ni(CClCCl2)(C6H4Me-2)(PMePh2)2

Guidance literature:
With n-butyllithium; In diethyl ether; dropwise addn. of an ethereal soln. of 2-tolyllithium, prepared from 2-bromotoluene and BuLi in diethyl ether, to a soln. of the Ni complex in dry diethyl ether at 0°C; stirring at room temp. overnight; performed under argon;; addn. of diethyl ether; the soln. was washed with H2O repeatedly and evapd. under vac.; recrystn. from acetone by addn. of CH3OH and concn.; repeated recrystn.; mixt. of syn- and anti-isomers obtained; elem. anal.;;
DOI:10.1016/0022-328X(83)87168-X
upstream raw materials:

2-methylphenyl bromide

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