3-(p-methoxyphenyl)-1,4,2-benzodiathizine

Base Information

• Chemical Name: 3-(p-methoxyphenyl)-1,4,2-benzodiathizine
• CAS No.: 77598-02-8
• Molecular Formula: C₁₄H₁₁NOS₂
• Molecular Weight: 273.379
• Mol file: 77598-02-8.mol

Synonyms:

Chemical Property of 3-(p-methoxyphenyl)-1,4,2-benzodiathizine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(p-methoxyphenyl)-1,4,2-benzodiathizine

There total 3 articles about 3-(p-methoxyphenyl)-1,4,2-benzodiathizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-(p-methoxyphenyl)-1,3-benzodithiol-2-yl azide (77598-10-8) → 3-(p-methoxyphenyl)-1,4,2-benzodiathizine (77598-02-8)

Guidance literature:

In benzene; for 3h; Heating;

DOI:10.1039/P19810000618

Reference yield:

2-(4-metoxyphenyl)benzo[d][1,3]dithiole (61666-75-9) → 3-(p-methoxyphenyl)-1,4,2-benzodiathizine (77598-02-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 83 percent / trityl tetrafluoroborate

2: 92 percent / sodium azide

3: 99 percent / benzene / 3 h / Heating

With sodium azide; trityl tetrafluoroborate; In benzene;

DOI:10.1039/P19810000618

Reference yield:

2-(p-methoxyphenyl)-1,3-benzodithiolylium tetrafluoroborate → 3-(p-methoxyphenyl)-1,4,2-benzodiathizine (77598-02-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / sodium azide

2: 99 percent / benzene / 3 h / Heating

With sodium azide; In benzene;

DOI:10.1039/P19810000618

upstream raw materials:

2-(p-methoxyphenyl)-1,3-benzodithiol-2-yl azide

2-(4-metoxyphenyl)benzo[d][1,3]dithiole