Technology Process of 3,6,1',4',6'-penta-O-acetyl-2,3'-anhydro-4-O-tosylsucrose
There total 8 articles about 3,6,1',4',6'-penta-O-acetyl-2,3'-anhydro-4-O-tosylsucrose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / pyridine
2: 69 percent / aq. 60percent acetic acid / 0.5 h / 50 °C
3: 1) pyridine, 2) pyridine / 1) 16 h, room temperature, 2) 48 h
With
pyridine; acetic acid;
DOI:10.1016/0008-6215(90)80136-Q
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 71.1 percent / p-toluenesulfonic acid / dimethylformamide / 1.5 h
2: 87 percent / pyridine
3: 69 percent / aq. 60percent acetic acid / 0.5 h / 50 °C
4: 1) pyridine, 2) pyridine / 1) 16 h, room temperature, 2) 48 h
With
pyridine; toluene-4-sulfonic acid; acetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80136-Q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 74.9 percent / 0.1M sodium hydroxide / 20 h / 100 °C
2: 71.1 percent / p-toluenesulfonic acid / dimethylformamide / 1.5 h
3: 87 percent / pyridine
4: 69 percent / aq. 60percent acetic acid / 0.5 h / 50 °C
5: 1) pyridine, 2) pyridine / 1) 16 h, room temperature, 2) 48 h
With
pyridine; sodium hydroxide; toluene-4-sulfonic acid; acetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80136-Q