3'-O-p-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis(2-cyanoethyl) ester

Base Information

• Chemical Name: 3'-O-p-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis(2-cyanoethyl) ester
• CAS No.: 81691-46-5
• Molecular Formula: C₇₇H₇₁N₁₇O₂₃P₂
• Molecular Weight: 1664.46

Synonyms:

Chemical Property of 3'-O-p-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis(2-cyanoethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 3'-O-p-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis(2-cyanoethyl) ester

There total 1 articles about 3'-O-p-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis(2-cyanoethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3'-O-p-methylbenzoyl-5'-O-monomethoxytrityl-N6-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N6-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N6-benzoyladenosine P1,P2-bis 2-cyanoethyl ester (81691-45-4) → 3'-O-p-methylbenzoyl-N6-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N6-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N6-benzoyladenosine P1,P2-bis(2-cyanoethyl) ester (81691-46-5)

Guidance literature:

With acetic acid; Heating;

Reference yield:

3'-O-p-methylbenzoyl-N6-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N6-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N6-benzoyladenosine P1,P2-bis(2-cyanoethyl) ester (81691-46-5) → adenylyl(2'-5')adenylyl(2'-5')adenosine (70062-83-8)

Guidance literature:

With pyridine; ammonia; triethylamine; Yield given. Multistep reaction; 1.) room temp., 16 h, 2.) methanol, room temp., 3 d;

upstream raw materials:

3'-O-p-methylbenzoyl-5'-O-monomethoxytrityl-N⁶-benzoyladenylyl-(2'->5')-3'-O-methylbenzoyl-N⁶-benzoyladenylyl-(2'->5')-2',3'-di-O-acetyl-N⁶-benzoyladenosine P¹,P²-bis 2-cyanoethyl ester

Downstream raw materials:

adenylyl(2'-5')adenylyl(2'-5')adenosine

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