C₆H₁₁CHC(CN)Ge(CH₃)3

Base Information

Chemical Name:C₆H₁₁CHC(CN)Ge(CH₃)3
CAS No.:101652-91-9
Molecular Formula:C₁₂H₂₁GeN
Molecular Weight:251.895
Hs Code.:

C<sub>6</sub>H<sub>11</sub>CHC(CN)Ge(CH<sub>3</sub>)3

Synonyms:

Suppliers and Price of C₆H₁₁CHC(CN)Ge(CH₃)3

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₆H₁₁CHC(CN)Ge(CH₃)3

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of C₆H₁₁CHC(CN)Ge(CH₃)3

There total 1 articles about C₆H₁₁CHC(CN)Ge(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101652-74-8
(trimethylgermyl)(trimethylsilyl)acetonitrile

: 2043-61-0
cyclohexanecarbaldehyde

: 101652-83-9
C₆H₁₁CHC(CN)Ge(CH₃)3

: 101652-91-9
C₆H₁₁CHC(CN)Ge(CH₃)3

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; BuLi in hexane was added at 0°C under N2 to a soln. of germylated acetonitrile in Et2O, mixt. was stirred for 1 h, a soln. of aldehyde in Et2O was added dropwise, stirring was continued for 2 h at the same temp.; total yield 77%, E/Z ratio 78:22; satd. aq. NH4Cl was added, mixt. extd. with benzene, ext. washed with water and satd. aq. NaCl, dried over anhyd. MgSO4, concd. in vacuo, residue chromd. on a SiO2 column (hexane-Et2O); elem. anals., isomers assigned on the basis of NMR and GLC data;
DOI:10.1021/om00137a023