(+/-)-zonarol

Base Information

• Chemical Name: (+/-)-zonarol
• CAS No.: 110715-67-8
• Molecular Formula: C₂₁H₃₀O₂
• Molecular Weight: 314.468
• Mol file: 110715-67-8.mol

Synonyms:

Chemical Property of (+/-)-zonarol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-zonarol

There total 55 articles about (+/-)-zonarol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(-)-ent-zonarol di-THP ether (478930-78-8) → (-)-ent-zonarol (39707-54-5,63813-82-1,110715-67-8)

Guidance literature:

With pyridinium p-toluenesulfonate; In ethanol; at 20 ℃; for 2h;

DOI:10.1080/00397910500377172

Reference yield: 75.0%

(+)-zonarone (39707-56-7) → (-)-ent-zonarol (39707-54-5,63813-82-1,110715-67-8)

Guidance literature:

With sodium dithionite; In tetrahydrofuran; water; for 0.5h; Heating;

DOI:10.1002/ejoc.200600389

Reference yield: 35.2%

(-)-zonarol dimethyl ether (108944-92-9) → (-)-ent-zonarol (39707-54-5,63813-82-1,110715-67-8)

Guidance literature:

With lithium-n-butanethiolate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 150 ℃; for 22h;

DOI:10.1002/bscb.19860950906

upstream raw materials:

(-)-zonarol dimethyl ether

Acetic acid [2,5-bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-((1S,2R,4aS,8aS)-2-hydroxy-2,5,5,8a-tetramethyl-decahydro-naphthalen-1-yl)-methyl ester

(-)-ent-zonarol di-THP ether

(+)-zonarone

Downstream raw materials:

(+)-zonarone