C₃₄H₄₉NO₆Si

Base Information

Chemical Name:C₃₄H₄₉NO₆Si
CAS No.:902454-60-8
Molecular Formula:C₃₄H₄₉NO₆Si
Molecular Weight:595.852
Hs Code.:

C<sub>34</sub>H<sub>49</sub>NO<sub>6</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₉NO₆Si

Chemical Property:

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Technology Process of C₃₄H₄₉NO₆Si

There total 1 articles about C₃₄H₄₉NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₈O₆Si

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 902454-60-8
C₃₄H₄₉NO₆Si

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 3h;
DOI:10.1039/b602021f

Reference yield:

: 902454-60-8
C₃₄H₄₉NO₆Si

: 902454-61-9
C₃₄H₄₉NO₇Si

Guidance literature:: C₃₄H₄₉NO₆Si; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

With (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Further stages.;
DOI:10.1039/b602021f

Reference yield:

: 902454-60-8
C₃₄H₄₉NO₆Si

: C₄₂H₅₆O₈Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: NaHMDS / tetrahydrofuran / 0.08 h / -78 °C

1.2: Davis oxaziridine / tetrahydrofuran / 0.08 h / -78 °C

2.1: 0.313 g / Mg(OMe)2 / 0.5 h / 0 °C

3.1: 86 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 25 °C

4.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

4.2: 92 percent / tetrahydrofuran; hexane / 1 h / -78 °C

5.1: LiCl / acetonitrile / 0.17 h / 25 °C

5.2: i-Pr₂NEt / acetonitrile / 0.17 h / 25 °C

5.3: 97 percent / acetonitrile / 36 h / 25 °C

6.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / 25 °C

6.2: 94 percent / tetrahydrofuran; toluene / -78 - 25 °C

7.1: 87 percent / PPTS / ethanol / 20 h / 45 °C

8.1: 79 percent / TsOH*H₂O / methanol / 16 h / 25 °C

9.1: 77 percent / Et₃N; 4-DMAP / CH₂Cl₂ / 16 h / 25 °C

10.1: 31 percent / (-)-(S,S)-diisopropyl D-tartrate; t-BuOOH; 4 Angstroem molecular sieves / Ti(Oi-Pr)4 / CH₂Cl₂; decane / 1.25 h / -25 °C

With 1H-imidazole; tert.-butylhydroperoxide; dmap; n-butyllithium; 4 A molecular sieve; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; toluene-4-sulfonic acid; magnesium methanolate; triethylamine; lithium chloride; titanium(IV) isopropylate; In tetrahydrofuran; methanol; decane; ethanol; hexane; dichloromethane; toluene; acetonitrile; 5.1: Horner-Wadsworth-Emmons olefination / 6.2: Wittig methylenation / 10.1: Katsuki-Sharpless epoxidation;
DOI:10.1039/b602021f