N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

Base Information

Chemical Name:N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine
CAS No.:129819-59-6
Molecular Formula:C₂₁H₂₁NO₃S
Molecular Weight:367.469
Hs Code.:

Synonyms:

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Chemical Property of N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

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Technology Process of N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

There total 7 articles about N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 129819-59-6
N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 56.5 percent / sodium methoxide / methanol / 0.08 h / 0 °C

2: 53.7 percent / LiAlH₄ / diethyl ether / 16 h / Heating

3: sodium acetate, acetic acid, sodium cyanoborohydride / methanol / 2 h / Ambient temperature

With lithium aluminium tetrahydride; sodium methylate; sodium acetate; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether;

Reference yield:

: 699-18-3,32782-45-9
2-(2-nitrovinyl)furan

: 129819-59-6
N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 53.7 percent / LiAlH₄ / diethyl ether / 16 h / Heating

2: sodium acetate, acetic acid, sodium cyanoborohydride / methanol / 2 h / Ambient temperature

With lithium aluminium tetrahydride; sodium acetate; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether;

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 129819-59-6
N-2-(2-furylethyl) α-phenylthio-1,3-benzodioxole-5-ethanamine

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / ZnCl₂ / acetic acid / 3 h / 60 °C

2: 88.4 percent / I₂ / acetonitrile / 0.33 h / 55 °C

3: HCl / Heating

4: 81 percent / diisobutylaluminum hydride / toluene / 0.67 h / -78 °C

5: sodium acetate, acetic acid, sodium cyanoborohydride / methanol / 2 h / Ambient temperature

With hydrogenchloride; iodine; sodium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; zinc(II) chloride; In methanol; acetic acid; toluene; acetonitrile;