trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃

Base Information

Chemical Name:trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃
CAS No.:399567-17-0
Molecular Formula:CF₃O₃S*C₃₉H₄₇N₅O₂PPd
Molecular Weight:904.299
Hs Code.:

trans-[Pd(C(=NBu-t)C<sub>6</sub>H<sub>4</sub>NH<sub>2</sub>-2-NO<sub>2</sub>-5)(CNBu-t)2(P(C<sub>6</sub>H<sub>5</sub>)3)]CF<sub>3</sub>SO<sub>3</sub>

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Chemical Property of trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃

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Technology Process of trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃

There total 1 articles about trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 399567-11-4
trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)Br(CNBu-t)2]

: 603-35-0
triphenylphosphine

: 73491-36-8
thallium(I) triflate

: 399567-17-0
trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃

: (P(C₆H₅)3Pd(CNC₄H₉)2)2⁽²⁺⁾*2CF₃SO₃^(1-)=(P(C₆H₅)3Pd(CNC₄H₉)2)2(CF₃SO₃)2

Guidance literature:: In acetone; PPh3 and Tl-salt were added to a soln. of complex in acetone, the suspn.was stirred for 15 min; filtered, evapd. to dryness, the residue was tritirated with diethyl ether, filtered, washed with diethyl ether and n-hexane, air-dried;
DOI:10.1021/om0104971

Reference yield:

: 399567-17-0
trans-[Pd(C(=NBu-t)C₆H₄NH₂-2-NO₂-5)(CNBu-t)2(P(C₆H₅)3)]CF₃SO₃

: (P(C₆H₅)3Pd(CNC₄H₉)2)2⁽²⁺⁾*2CF₃SO₃^(1-)=(P(C₆H₅)3Pd(CNC₄H₉)2)2(CF₃SO₃)2

Guidance literature:: In not given; a soln. in acetone or CH2Cl2 was left standing for 24 h at room temp.; diethyl ether was slowly added, the mixt. was left overnight in refrigerator;
DOI:10.1021/om0104971