Technology Process of C68H112N2O8
There total 8 articles about C68H112N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 12 h / Reflux
2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 18 h / Reflux
2.2: 12 h / 20 °C
3.1: hydrogen bromide / water / 24 h / Reflux
4.1: ethanol / 12 h / Reflux
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; potassium carbonate;
In
diethyl ether; ethanol; water; acetone;
DOI:10.1016/j.tetlet.2013.04.071
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C
2: nitric acid; sodium nitrite / dichloromethane / 1 h / 20 °C
3: palladium 10% on activated carbon / tetrahydrofuran / 12 h / 20 °C
4: ethanol / 12 h / Reflux
With
palladium 10% on activated carbon; nitric acid; potassium carbonate; potassium iodide; sodium nitrite;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.04.071