((CH₃)3C₆H₂N(CH₂)2N(CH₃)3C₆H₂Sn)2

Base Information

• Chemical Name: ((CH₃)3C₆H₂N(CH₂)2N(CH₃)3C₆H₂Sn)2
• CAS No.: 1083333-49-6
• Molecular Formula: C₄₀H₅₂N₄Sn₂
• Molecular Weight: 826.3
• Mol file: 1083333-49-6.mol

Synonyms:

Chemical Property of ((CH₃)3C₆H₂N(CH₂)2N(CH₃)3C₆H₂Sn)2

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of ((CH₃)3C₆H₂N(CH₂)2N(CH₃)3C₆H₂Sn)2

There total 1 articles about ((CH₃)3C₆H₂N(CH₂)2N(CH₃)3C₆H₂Sn)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

tin(ll) chloride + N,N'-dimesityl-1,2-ethanediamine (134030-21-0) → ((CH3)3C6H2N(CH2)2N(CH3)3C6H2Sn)2 (1083333-49-6)

Guidance literature:

With C₄H₉Li; In diethyl ether; hexane; (Ar, glovebox); 1.6 M soln. of n-BuLi in hexane was added to soln. of diimine in Et2O at 0°C, stirred for 2 h, suspn. of SnCl2 in Et2O was added at -78°C, warmed to room temp., stirred for 2 h; evapd., extd. with nhexane, extract was filtered, filtrate concd. in vac, left at -18°C fo crystn., elem. anal.;

DOI:10.1021/ic801479g

upstream raw materials:

N,N'-dimesityl-1,2-ethanediamine