5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)

Base Information

Chemical Name:5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)
CAS No.:83182-07-4
Molecular Formula:C₁₀H₁₆OS₂
Molecular Weight:216.368
Hs Code.:

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Chemical Property of 5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)

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Technology Process of 5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)

There total 1 articles about 5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 15732-74-8
dispiro-1,2';3,2'-(5,5-dimethylcyclohexane)

: 83182-07-4
5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)

: 3-(2-Mercapto-ethylsulfanyl)-5,5-dimethyl-cyclohex-2-enone

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; for 1h; Product distribution; Ambient temperature; various solvents, timmes and sonication;

Reference yield:

: 83182-07-4
5,5-dimethylcyclohexane-1,3-dione 1-(ethylene dithioacetal)

: 5-carbamoyloxy-3,3-dimethylcyclohexanone dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaBH₄ / ethanol / 1 h

2: 2.) NH₃ gas / 1.) Py, 4 h

3: 1.) phenylseleninic anhydride, propylene oxide, 2.) TsOH / 1.) CH₂Cl₂, 4 h, 2.) MeOH, 1 h, room temperature

With sodium tetrahydroborate; benzeneseleninic anhydride; ammonia; toluene-4-sulfonic acid; methyloxirane; In ethanol;