Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

Base Information

Chemical Name:Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2
CAS No.:98838-50-7
Molecular Formula:C₅₀H₃₈N₂O₂P₂Pt
Molecular Weight:955.891
Hs Code.:

Pt((C<sub>6</sub>H<sub>5</sub>)2PC<sub>6</sub>H<sub>4</sub>C(O)NC<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

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Technology Process of Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

There total 2 articles about Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98838-49-4
trans-dichlorobis(o-(diphenylphosphino)-N-phenylbenzamide)platinum(II)

: 98838-50-7,98919-88-1
Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

Guidance literature:: With sodium methylate; In acetonitrile; suspending Pt complex and excess of sodium methoxide in dry acetonitrile; stirring under dry atmosphere for 3 days at ambient temp.;; filtration; washing with CH2Cl2; evapn. of combined filtrates to dryness; recrystn. from CH2Cl2/hexane; washing with hexane; drying in vac.; elem. anal.;;

Reference yield: 68.0%

: 98838-49-4
trans-dichlorobis(o-(diphenylphosphino)-N-phenylbenzamide)platinum(II)

: 98838-50-7,98919-88-1
Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In acetonitrile; suspending Pt complex and excess of Dabco in dry acetonitrile; refluxing for 1 h under N2; cooling to room temp.;; removal of solvent; dissolving in CH2Cl2; filtration; extn. with aq. NaCl; drying organic layer over MgSO4; reduction of volume; addn. of (C2H5)2O; pptn.; filtration; washing with (C2H5)2O; drying in vac.; recrystn.from CH2Cl2/hexane; elem. anal.;;

Reference yield: 90.0%

: 98838-50-7,98919-88-1
Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)2

: 76-05-1
trifluoroacetic acid

: 99642-29-2
{Pt((C₆H₅)2PC₆H₄C(O)NC₆H₅)((C₆H₅)2PC₆H₄C(O)NHC₆H₅)(CF₃CO₂)}*H⁽¹⁺⁾*CF₃CO₂^(1-)

Guidance literature:: In dichloromethane; soln. of starting complex in CH2Cl2 treated with excess CF3COOH, reacted for 10 min; filtered, evapd., stirred with Et2O, powder filtered, washed with Et2O, dried in vac.; elem. anal.;
DOI:10.1021/om00133a024