(OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

Base Information

Chemical Name:(OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl
CAS No.:92922-75-3
Molecular Formula:C₁₈H₁₄BrClMnO₅P
Molecular Weight:511.575
Hs Code.:

(OC)4MnBrP(C<sub>6</sub>H<sub>5</sub>)2OCH<sub>2</sub>CH<sub>2</sub>Cl

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Chemical Property of (OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

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Technology Process of (OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

There total 1 articles about (OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14516-54-2
bromopentacarbonylmanganese(I)

: 35411-11-1
β-chloroethyl diphenylphosphite

: 92922-75-3
(OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

Guidance literature:: In hexane; equimolar amts. of educts warmed for 2 h at 45°C, heated to 60°C for 0.5 h; filtered, evapd. of solvent, recrystd. from hexane or chromy., elem. anal.;

Reference yield: 66.0%

: 92922-75-3
(OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

: 97429-04-4
a-bromo-bdf-tricarbonyl-c-[(2-chlorethoxy)diphenylphosphane]-e-(triphenylphosphane)manganese

Guidance literature:: With triphenylphosphine; In toluene; byproducts: CO; under N2 atmosphere; heating of a stirred soln. of the Mn compd. and the ligand at 85°C for 15 h;; filtration of the hot soln.; evapn.; dissoln. in CHCl3; pptn. by addn. of petroleum ether at -30°C; recrystn. from CHCl3/hexane; elem. anal.;;

Reference yield: 40.0%

: 92922-75-3
(OC)4MnBrP(C₆H₅)2OCH₂CH₂Cl

: (OC)4(MnP(C₆H₅)2OCH₂CH₂)

Guidance literature:: With sodium amalgam; In diethyl ether; compounds mixed at 0°C, then cooled to -15°C; filtered in Ar at 0°C, evapd. of solvent at -30°C in high vac., extd. with n-pentane, filtered at -70°C, evapd. of solvent at -30°C in high vac., chromy., recrystd. from n-pentane at -80°C, elem. anal.;