Technology Process of C60H50N4
There total 7 articles about C60H50N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; 4-methoxy-phenol;
In
toluene;
for 48h;
Reflux;
Molecular sieve;
DOI:10.1021/om200193r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / tetrahydrofuran
1.2: 3 h / -45 - 20 °C
2.1: potassium phosphate monohydrate / tetrahydrofuran; water / Inert atmosphere
2.2: 12 h / Reflux; Inert atmosphere
3.1: toluene-4-sulfonic acid; 4-methoxy-phenol / toluene / 48 h / Reflux; Molecular sieve
With
potassium phosphate monohydrate; toluene-4-sulfonic acid; magnesium; 4-methoxy-phenol;
In
tetrahydrofuran; water; toluene;
2.1: Suzuki coupling / 2.2: Suzuki coupling;
DOI:10.1021/om200193r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium phosphate monohydrate / tetrahydrofuran; water / Inert atmosphere
1.2: 12 h / Reflux; Inert atmosphere
2.1: toluene-4-sulfonic acid; 4-methoxy-phenol / toluene / 48 h / Reflux; Molecular sieve
With
potassium phosphate monohydrate; toluene-4-sulfonic acid; 4-methoxy-phenol;
In
tetrahydrofuran; water; toluene;
1.1: Suzuki coupling / 1.2: Suzuki coupling;
DOI:10.1021/om200193r
