C₂₁H₂₀N₆OS

Base Information

Chemical Name:C₂₁H₂₀N₆OS
CAS No.:1602732-17-1
Molecular Formula:C₂₁H₂₀N₆OS
Molecular Weight:404.495
Hs Code.:

C<sub>21</sub>H<sub>20</sub>N<sub>6</sub>OS

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₀N₆OS

Chemical Property:

Purity/Quality:

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Technology Process of C₂₁H₂₀N₆OS

There total 5 articles about C₂₁H₂₀N₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1602730-52-8
C₁₆H₁₇N₃O₃

: 1602732-17-1
C₂₁H₂₀N₆OS

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2: methanol / 20 °C

3: tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; copper(II) sulfate; sodium L-ascorbate / dimethyl sulfoxide; water / 24 h / 20 °C

With lithium aluminium tetrahydride; copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; 2: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.bmcl.2014.03.026

Reference yield:

: 1602730-56-2
2-((3-formylphenyl)amino)benzamide

: 1602732-17-1
C₂₁H₂₀N₆OS

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 20 °C

2: tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; copper(II) sulfate; sodium L-ascorbate / dimethyl sulfoxide; water / 24 h / 20 °C

With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In methanol; water; dimethyl sulfoxide; 1: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.bmcl.2014.03.026

Reference yield:

: 618-51-9
3-Iodobenzoic acid

: 1602732-17-1
C₂₁H₂₀N₆OS

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / dichloromethane / Reflux

2: triethylamine / dichloromethane / 20 °C

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; potassium carbonate / tert-butyl alcohol / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

5: methanol / 20 °C

6: tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; copper(II) sulfate; sodium L-ascorbate / dimethyl sulfoxide; water / 24 h / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; XPhos; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol; 3: |Buchwald-Hartwig Coupling / 5: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.bmcl.2014.03.026