2,9,16,23-Tetraazanonacosanedioic acid, 8,15,22-trioxo-, 1-(phenylmethyl) ester

Base Information

Chemical Name:2,9,16,23-Tetraazanonacosanedioic acid, 8,15,22-trioxo-, 1-(phenylmethyl) ester
CAS No.:117025-58-8
Molecular Formula:C₃₂H₅₂N₄O₇
Molecular Weight:604.787
Hs Code.:
Mol file:117025-58-8.mol

Synonyms:

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Chemical Property of 2,9,16,23-Tetraazanonacosanedioic acid, 8,15,22-trioxo-, 1-(phenylmethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2,9,16,23-Tetraazanonacosanedioic acid, 8,15,22-trioxo-, 1-(phenylmethyl) ester

There total 6 articles about 2,9,16,23-Tetraazanonacosanedioic acid, 8,15,22-trioxo-, 1-(phenylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49701-55-5
13-benzyloxycarbonylamino-8-oxo-7-azatridecanoic acid

: 117025-58-8
[4]6-benzyloxycarbonylamino-lin-tri[1=>6]hexanoylamino-hexanoic acid

Guidance literature:: With tetrahydrofuran; chloroformic acid ethyl ester; triethylamine; anschliessend Behandeln mit 6-<6-Amino-hexanoylamino>-hexansaeure und wss. NaOH;

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 117025-58-8
[4]6-benzyloxycarbonylamino-lin-tri[1=>6]hexanoylamino-hexanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: chlorocarbonic acid benzyl ester; aqueous NaOH

2: triethylamine; chlorocarbonic acid ethyl ester; toluene / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid ethyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

4: triethylamine; chlorocarbonic acid ethyl ester; DMF / anschliessend Behandeln mit 6-Amino-hexansaeure-aethylester-hydrochlorid in CH₂Cl₂

5: aq.-ethanolic NaOH

With tetrahydrofuran; sodium hydroxide; chloroformic acid ethyl ester; benzyl chloroformate; triethylamine; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 117025-58-8
[4]6-benzyloxycarbonylamino-lin-tri[1=>6]hexanoylamino-hexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; chlorocarbonic acid ethyl ester; toluene / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

2: triethylamine; chlorocarbonic acid ethyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid ethyl ester; DMF / anschliessend Behandeln mit 6-Amino-hexansaeure-aethylester-hydrochlorid in CH₂Cl₂

4: aq.-ethanolic NaOH

With tetrahydrofuran; sodium hydroxide; chloroformic acid ethyl ester; triethylamine; N,N-dimethyl-formamide; toluene;