Technology Process of C18H20N2O2
There total 5 articles about C18H20N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
Inert atmosphere;
Cooling;
DOI:10.1002/ejoc.201100274
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; isobutyl chloroformate / dichloromethane / Inert atmosphere; Cooling
1.2: 20 °C / Inert atmosphere; Cooling
2.1: trifluoroacetic acid / dichloromethane / Inert atmosphere
3.1: potassium carbonate / acetonitrile / Inert atmosphere; Heating
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Inert atmosphere; Cooling
With
potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; isobutyl chloroformate;
In
dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201100274
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; isobutyl chloroformate / dichloromethane / Inert atmosphere; Cooling
1.2: 20 °C / Inert atmosphere; Cooling
2.1: trifluoroacetic acid / dichloromethane / Inert atmosphere
3.1: potassium carbonate / acetonitrile / Inert atmosphere; Heating
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Inert atmosphere; Cooling
With
potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; isobutyl chloroformate;
In
dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201100274
