(1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate

Base Information

• Chemical Name: (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate
• CAS No.: 1167426-80-3
• Molecular Formula: C₂₉H₄₃N₅O₁₁S
• Molecular Weight: 669.753

Synonyms:

Chemical Property of (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate

Chemical Property:

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Technology Process of (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate

There total 1 articles about (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(nitrooxy)hexanoic acid (74754-55-5) + (S)-3-(tert-butylamino)-1-(4-morpholino-1,2,5-thiadiazol-3-yloxy)propan-2-yl 2-(chloromethyl)-4,6-dimethoxybenzoate (1167426-79-0) → (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate (1167426-80-3)

Guidance literature:

With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 8h;

DOI:10.1016/j.bmcl.2009.03.111

Reference yield:

(1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate (1167426-80-3) + maleic acid (110-16-7,26099-09-2) → (1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate maleate (1167426-81-4)

Guidance literature:

In ethyl acetate; for 0.5h;

DOI:10.1016/j.bmcl.2009.03.111

upstream raw materials:

6-(nitrooxy)hexanoic acid

(S)-3-(tert-butylamino)-1-(4-morpholino-1,2,5-thiadiazol-3-yloxy)propan-2-yl 2-(chloromethyl)-4,6-dimethoxybenzoate

Downstream raw materials:

(1S)-3-(tert-butylamino)-1-{[(4-morpholin-4-yl-1,2,5-thiadiazol-3-yl)oxy]methyl}ethyl 2,4-dimethoxy-6-({[6-(nitroxy)hexanoyl]oxy}methyl)benzoate maleate

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