6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

Base Information

Chemical Name:6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine
CAS No.:118971-38-3
Molecular Formula:C₁₈H₉ClN₈S
Molecular Weight:404.842
Hs Code.:

6-o-chlorophenyl-3-mercaptobenzo<f>-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo<e>-as-triazine

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Chemical Property of 6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

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Technology Process of 6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

There total 10 articles about 6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 118971-32-7
2-o-chlorophenyl-6-hydrazinobenzo-v-triazolo<4,5-h>benzo-as-triazine

: 118971-38-3
6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

Guidance literature:: With pyridine; carbon disulfide; for 1.5h; Heating;

Reference yield:

: 118971-21-4
2-o-chlorophenyl-2H-naphtho<1,2-d>-v-triazole-4,5-quinone

: 118971-38-3
6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

Guidance literature:: Multi-step reaction with 5 steps

1: 61 percent / acetic acid / 0.5 h / Heating

2: 34 percent / 5percent aq. KOH / 1 h / Heating

3: 91 percent / POCl₃ / 1.5 h / 140 °C

4: 74 percent / 99percent N₂H₄*H₂O / 0.5 h / Heating

5: 57 percent / CS₂/pyridine / 1.5 h / Heating

With pyridine; carbon disulfide; potassium hydroxide; hydrazine hydrate; trichlorophosphate; In acetic acid;

Reference yield:

: 95-51-2
o-chloroaniline

: 118971-38-3
6-o-chlorophenyl-3-mercaptobenzo-v-triazolo<4,5-h>-s-triazolo<4,3-b>benzo-as-triazine

Guidance literature:: Multi-step reaction with 7 steps

1: 1.)NaNO₂/aq. HCl 2.)NaOAc / 1.)below 5 deg C 2.)EtOH, 40 deg C

2: 61 percent / CrO₃/Ac₂O / acetic acid

3: 61 percent / acetic acid / 0.5 h / Heating

4: 34 percent / 5percent aq. KOH / 1 h / Heating

5: 91 percent / POCl₃ / 1.5 h / 140 °C

6: 74 percent / 99percent N₂H₄*H₂O / 0.5 h / Heating

7: 57 percent / CS₂/pyridine / 1.5 h / Heating

With pyridine; chromium(VI) oxide; hydrogenchloride; carbon disulfide; potassium hydroxide; sodium acetate; acetic anhydride; hydrazine hydrate; sodium nitrite; trichlorophosphate; In acetic acid;