Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3)⁽¹⁺⁾*PF₆^(1-)=(Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3))PF₆

Base Information

• Chemical Name: Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3)⁽¹⁺⁾*PF₆^(1-)=(Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3))PF₆
• CAS No.: 1345820-46-3
• Molecular Formula: C₈₂H₇₈N₉Zn*F₆P
• Molecular Weight: 1399.94

Synonyms:

Chemical Property of Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3)⁽¹⁺⁾*PF₆^(1-)=(Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3))PF₆

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Technology Process of Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3)⁽¹⁺⁾*PF₆^(1-)=(Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3))PF₆

There total 1 articles about Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3)⁽¹⁺⁾*PF₆^(1-)=(Zn(N₄C₂₀H₃(C₂H₅)8NC₅H₄C₂₀H₁₀N₄(C₆H₄CH₃)3))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(2,3,7,8,12,13,17,18-octaethylporphyrinato)zinc(II) (17632-18-7) + 5-(p-pyridyl)-10,15,20-tris(p-tolyl)porphyrin → Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3)(1+)*PF6(1-)=(Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3))PF6 (1345820-46-3)

Guidance literature:

With tetraethylammonium hexafluorophosphate; 2,6-lutidine; In 1,2-dichloro-ethane; acetonitrile; Electrolysis; under Ar; Zn compd. and porphyrin dissolved in 1,2-dichloroethane-MeCN soln. contg. Et4NPF6; lutidine added; subjected to electrolysis at 0.75 V(vs. satd. calomel electrode) for 24 h with stirring; solvent removed; dissolved in 1,2-dichloroethane; soln. washed with H2O;org. layer concd.; chromd. (silica, CH2Cl2, CH2Cl2-MeOH 99.75:0.25); th ird fraction collected; solvent removed;

DOI:10.1039/c1nj20177h

Reference yield:

Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3)(1+)*PF6(1-)=(Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3))PF6 (1345820-46-3) → Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3)

Guidance literature:

With Bu₄NPF₆; In 1,2-dichloro-ethane; Electrochem. Process; under Ar; Zn compd. in 1,2-dichloroethane in presence of Bu4NPF6 electrochemically reduced at -0.74 V (vs. Ag/AgCl); not isolated; monitored by UV-vis spectra;

DOI:10.1039/c1nj20177h

Reference yield:

Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3)(1+)*PF6(1-)=(Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3))PF6 (1345820-46-3) → Zn(N4C20H3(C2H5)8NC5H4C20H10N4(C6H4CH3)3)(2+)

Guidance literature:

With Bu₄NPF₆; In 1,2-dichloro-ethane; Electrochem. Process; under Ar; Zn compd. in 1,2-dichloroethane in presence of Bu4NPF6 electrochemically oxidized at 0.95 V (vs. Ag/AgCl); not isolated; monitored by UV-vis spectra;

DOI:10.1039/c1nj20177h

upstream raw materials:

(2,3,7,8,12,13,17,18-octaethylporphyrinato)zinc(II)

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