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Technology Process of C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2

C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2

Base Information
  • Chemical Name:C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2
  • CAS No.:1352228-57-9
  • Molecular Formula:C93H116N2P4Pt2S5
  • Molecular Weight:1936.34
  • Hs Code.:
C<sub>4</sub>HS(C<sub>4</sub>HSC<sub>6</sub>H<sub>13</sub>C<sub>4</sub>H<sub>2</sub>SCC)2(CN<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)C<sub>14</sub>H<sub>8</sub>)[Pt(C<sub>6</sub>H<sub>5</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2]2

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Chemical Property of C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2
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Technology Process of C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2

There total 1 articles about C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

trans-bis(triethylphosphino)phenylchloro platinum(II)

trans-bis(triethylphosphino)phenylchloro platinum(II)

C<sub>4</sub>HS(C<sub>4</sub>HSC<sub>6</sub>H<sub>13</sub>C<sub>4</sub>H<sub>2</sub>SCCH)2(CN<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)C<sub>14</sub>H<sub>8</sub>)
1352135-50-2

C4HS(C4HSC6H13C4H2SCCH)2(CN2(C6H5)C14H8)

C<sub>4</sub>HS(C<sub>4</sub>HSC<sub>6</sub>H<sub>13</sub>C<sub>4</sub>H<sub>2</sub>SCC)2(CN<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)C<sub>14</sub>H<sub>8</sub>)[Pt(C<sub>6</sub>H<sub>5</sub>)(P(C<sub>2</sub>H<sub>5</sub>)3)2]2
1352228-57-9

C4HS(C4HSC6H13C4H2SCC)2(CN2(C6H5)C14H8)[Pt(C6H5)(P(C2H5)3)2]2

Guidance literature:
copper(l) iodide; In dichloromethane; triethylamine; to stirred soln. of thiophene deriv. and Pt complex in NEt3 added CuI; stirred at room temp. overnight under N2; volatiles removed in vacuo; residue dissolved in CH2Cl2; purified by SiO2 eluting with CH2Cl2/hexane; elem.anal.;
DOI:10.1016/j.jorganchem.2011.07.005
upstream raw materials:

C4HS(C4HSC6H13C4H2SCCH)2(CN2(C6H5)C14H8)

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