YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2)

Base Information

Chemical Name:YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2)
CAS No.:1367453-00-6
Molecular Formula:C₄₄H₆₀IN₂O₂SiYb
Molecular Weight:977.003
Hs Code.:

YbI(THF)2(Ph<sub>2</sub>Si(N(2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>))2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2)

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Technology Process of YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2)

There total 1 articles about YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 13813-44-0
ytterbium(III) iodide

: 587023-11-8
C₃₇H₄₆N₂

: 1367453-00-6
YbI(THF)2(Ph₂Si(N(2,6-iPr₂C₆H₃))2)

Guidance literature:: With KH; In tetrahydrofuran; Schlenk technique; soln. of Ph2Si(2,6-iPr2C6H3NH)2 in thf slowly added to stirred suspn. of KH; mixt. stirred for 2 h at room temp.; filtered, treated with YbI3 at room temp. for 4 h; solvent removed under reduced pressure, Et2O added; filtered, reduced to5 mL, kept for several d at room temp.; elem. anal.;
DOI:10.1002/ejic.201101199