1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Base Information

Chemical Name:1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride
CAS No.:74243-35-9
Molecular Formula:C₂₀H₂₄N₂O₂*ClH
Molecular Weight:360.884
Hs Code.:

Synonyms:

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Chemical Property of 1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Chemical Property:

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Technology Process of 1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

There total 3 articles about 1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61-54-1
tryptamine

: 74243-35-9
1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80.6 percent / silver oxide / dioxane / 0.33 h / Ambient temperature

2: 1.) phosphorous oxychloride; 2.) sodium borohydride / 1.) benzene, 3 h., reflux; 2.) methanol, 10 min., room temp.

With sodium tetrahydroborate; silver(l) oxide; trichlorophosphate; In 1,4-dioxane;
DOI:10.1016/S0040-4020(01)98879-9

Reference yield:

: 74207-04-8
methyl cis-6-<(diazomethyl)carbonyl>-3-cyclohexene-1-carboxylate

: 74243-35-9
1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80.6 percent / silver oxide / dioxane / 0.33 h / Ambient temperature

2: 1.) phosphorous oxychloride; 2.) sodium borohydride / 1.) benzene, 3 h., reflux; 2.) methanol, 10 min., room temp.

With sodium tetrahydroborate; silver(l) oxide; trichlorophosphate; In 1,4-dioxane;
DOI:10.1016/S0040-4020(01)98879-9

Reference yield:

: 74207-05-9
(1S,6S)-6-{[2-(1H-Indol-3-yl)-ethylcarbamoyl]-methyl}-cyclohex-3-enecarboxylic acid methyl ester

: 74207-07-1,74243-36-0,111561-00-3
dihydrooxoyohimbane

: 74243-35-9
1-(1,2,3,6-tetrahydro-2-methoxycarbonylbenzyl)-1,2,3,4-tetrahydro-β-carboline hydrochloride

Guidance literature:: With sodium tetrahydroborate; trichlorophosphate; Yield given. Multistep reaction. Yields of byproduct given; 1.) benzene, 3 h., reflux; 2.) methanol, 10 min., room temp.;
DOI:10.1016/S0040-4020(01)98879-9