C₂₄H₃₀O₆

Base Information

Chemical Name:C₂₄H₃₀O₆
CAS No.:1365268-52-5
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₄H₃₀O₆

Chemical Property:

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Technology Process of C₂₄H₃₀O₆

There total 19 articles about C₂₄H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1365268-38-7
C₂₄H₃₀O₆

: 1365268-51-4
C₂₄H₃₀O₆

: 1365268-52-5
C₂₄H₃₀O₆

: 1365268-39-8
C₂₄H₃₀O₆

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 0 ℃; for 0.833333h; diastereoselective reaction;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-32-1
C₄₁H₅₄O₆Si

: 1365268-51-4
C₂₄H₃₀O₆

: 1365268-52-5
C₂₄H₃₀O₆

: 1365268-39-8
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

4.2: -78 °C

5.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

6.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

7.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

8.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

9.1: hydrogenchloride; water / tetrahydrofuran / 45 °C

10.1: Dess-Martin periodane / dichloromethane / 20 °C

11.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

12.1: methanol / benzene / 20 °C

13.1: lithium diisopropyl amide / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.83 h / -78 - 0 °C

With hydrogenchloride; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; pig liver esterase; 2-methyl-but-2-ene; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; diisobutylaluminium hydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; tert-butyl alcohol; benzene; 10.1: Dess-Martin oxidation / 11.1: Pinnick oxidation / 13.1: transannular cascade Michael reaction;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-31-0
C₂₂H₃₀O₃

: 1365268-51-4
C₂₄H₃₀O₆

: 1365268-52-5
C₂₄H₃₀O₆

: 1365268-39-8
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 17 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C

1.2: -78 - 20 °C

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

2.2: 0 °C

2.3: -78 °C

3.1: 1H-imidazole / dichloromethane / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

5.1: diisobutylaluminium hydride / dichloromethane / -78 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

7.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

8.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

8.2: -78 °C

9.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

10.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

11.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

12.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

13.1: hydrogenchloride; water / tetrahydrofuran / 45 °C

14.1: Dess-Martin periodane / dichloromethane / 20 °C

15.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

16.1: methanol / benzene / 20 °C

17.1: lithium diisopropyl amide / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.83 h / -78 - 0 °C

With 1H-imidazole; hydrogenchloride; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; pig liver esterase; 2-methyl-but-2-ene; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; tert-butyl alcohol; benzene; 14.1: Dess-Martin oxidation / 15.1: Pinnick oxidation / 17.1: transannular cascade Michael reaction;
DOI:10.1016/j.tetlet.2012.01.058