1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

Base Information

Chemical Name:1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol
CAS No.:99562-43-3
Molecular Formula:C₁₀H₈F₆OS
Molecular Weight:290.229
Hs Code.:

Synonyms:

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Chemical Property of 1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

Chemical Property:

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Technology Process of 1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

There total 1 articles about 1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₂₁F₆OSSn^(1-)*K⁽¹⁺⁾

: 99562-43-3
1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

Guidance literature:: With air;
DOI:10.1021/ja00059a056

Reference yield:

: potassium tetrachloroplatinate

: 99562-43-3
1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

: 99604-04-3,99569-07-0
Pt(S(C₆H₅)OC(CF₃)2CH₂)2

Guidance literature:: With potassium hydroxide; In ethanol; dichloromethane; byproducts: KCl; To a soln. of K2PtCl4 in CH2Cl2 ligand is added followed by an ethanolic soln. of KOH, mixt. is stirred 6 days at 25°C.; KCl is removed, then solvents are removed by vac. evapn. at 25°C, residue is extd. with warm acetone, soln. is reduced in volume and chloroform is added, ppt. is recrystd. from acetone/chloroform, mixt. of syn-/anti-isomers, monitored by NMR.;

Reference yield:

: 99562-43-3
1,1,1,3,3,3-hexafluoro-2-<(phenylthio)methyl>-2-propanol

: palladium dichloride

: 99569-09-2,99604-30-5,99604-06-5
Pd(S(C₆H₅)OC(CF₃)2CH₂)2

Guidance literature:: With potassium hydroxide; In ethanol; N,N-dimethyl-formamide; byproducts: KCl; To a soln. of PdCl2 in DMF the ligand is added followed by addn. of a soln. of KOH in ethanol.; Ppt. of KCl is removed by centrifugation and the resulted soln. is stirred for 15 h, solvents are removed by vac. evapn.at 25°C, residueis extd. with acetone and recrystd. from ether, mixt. of trans/cis-syn/cis-anti (monitored by NMR).;