2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol

Base Information

• Chemical Name: 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol
• CAS No.: 1370548-95-0
• Molecular Formula: C₁₄H₁₈O₃
• Molecular Weight: 234.295

Synonyms:

Chemical Property of 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol

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Technology Process of 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol

There total 2 articles about 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-one (1370548-94-9) → 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol (1370548-95-0) + 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol + 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃; for 1.33333h; optical yield given as %ee; diastereoselective reaction; Inert atmosphere;

DOI:10.1039/c2ob07095b

Reference yield:

2-methoxy-(3-methoxy-2-vinyl-phenyl)-but-3-en-1-ol → 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol (1370548-95-0) + 2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.33 h / -78 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c2ob07095b

Reference yield:

2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-ol (1370548-95-0) + (S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride (39637-99-5,20445-33-4) → C24H25F3O5 (1370549-06-6) + C24H25F3O5

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 12h; optical yield given as %de; Inert atmosphere;

DOI:10.1039/c2ob07095b

upstream raw materials:

2-methoxy-1(3-methoxy-2-vinyl-phenyl)-but-3-ene-1-one

Downstream raw materials:

C₂₄H₂₅F₃O₅

C₂₄H₂₅F₃O₅

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