Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2))

Base Information

• Chemical Name: Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2))
• CAS No.: 1378939-05-9
• Molecular Formula: C₃₁H₂₈N₄OP₂PdS
• Molecular Weight: 673.023
• Mol file: 1378939-05-9.mol

Synonyms:

Chemical Property of Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2))

There total 1 articles about Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-(1H-pyrrol-2-ylmethylene)hydrazinecarbothioamide (5451-36-5,433215-03-3) + (bis(diphenylphosphino)methane)palladium(II) dichloride (38425-01-3) → Pt(κ(3)-N,N,S-pyrrole-2-carbaldehyde thiosemicarbazone(-1H))(κ(1)-P-PPh2CH2P(O)Ph2)) (1378939-05-9)

Guidance literature:

With N(C₂H₅)3; In toluene; byproducts: (C2H5)3NHCl; thiosemicarbazone deriv. added to suspn. of Pd complex in toluene, NEt3 added, mixt. stirred for 4 h; soln. filtered, filtrate allowed to evap. at room temp.; elem. anal.;

DOI:10.1002/zaac.201200012

upstream raw materials:

2-(1H-pyrrol-2-ylmethylene)hydrazinecarbothioamide

(bis(diphenylphosphino)methane)palladium(II) dichloride