cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃

Base Information

Chemical Name:cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃
CAS No.:334912-14-0
Molecular Formula:CF₃O₃S*C₃₄H₄₃N₂O₃PdS₂
Molecular Weight:847.349
Hs Code.:

cis-[Pd<sub>2</sub>(k2-C,S-CH(STol-p)(C<sub>6</sub>H(STol-p-2)(OMe)3-3,4,5))2(CNC<sub>4</sub>H<sub>9</sub>-tert)2]OSO<sub>2</sub>CF<sub>3</sub>

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Chemical Property of cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃

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Technology Process of cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃

There total 1 articles about cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 334912-05-9
[Pd2(k2-C,S-CH(STol-p)(C6H(STol-p-2)(OMe)3-3,4,5))2(μ-I)2]

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 73491-36-8
thallium(I) triflate

: 334912-14-0
cis-[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))2(CNC₄H₉-tert)2]OSO₂CF₃

Guidance literature:: In dichloromethane; complex was reacted with Tl-salt in CH2Cl2 for 15 min, NC-compound was added, the mixt. was stirred for 2 h; fileterd, concd., Et2O was added, filetered, the solid was washed with Et2O and dried with air, then in an oven at 70°C for 3 h, 3 d in vac. desiccator over P2O5; elem. anal.;
DOI:10.1021/om0008981