Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-yl>methylhydrazon-5'-oxid

Base Information

• Chemical Name: Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-yl>methylhydrazon-5'-oxid
• CAS No.: 86213-85-6
• Molecular Formula: C₂₆H₃₀N₈OP₂
• Molecular Weight: 532.525

Synonyms:

Chemical Property of Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-yl>methylhydrazon-5'-oxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-yl>methylhydrazon-5'-oxid

There total 8 articles about Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-yl>methylhydrazon-5'-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ5,10λ5-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole (63148-50-5) → Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-yl>methylhydrazon-5'-oxid (86213-85-6,86286-46-6,344913-13-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 87 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 93 percent / Et₃N / benzene / 12 h

3: 88 percent / Et₃N / benzene

4: 68 percent / Et₃N / benzene / 1 h

5: CHCl₃

With triethylamine; In dichloromethane; chloroform; benzene;

Reference yield:

N1-methylbenzamidrazone hydrochloride (28705-52-4) → Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-yl>methylhydrazon-5'-oxid (86213-85-6,86286-46-6,344913-13-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 87 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 93 percent / Et₃N / benzene / 12 h

3: 88 percent / Et₃N / benzene

4: 68 percent / Et₃N / benzene / 1 h

5: CHCl₃

With triethylamine; In dichloromethane; chloroform; benzene;

Reference yield:

P,P-dichlorophenylphosphine oxide (824-72-6) → Aceton-<9,10-dihydro-1,9-dimethyl-3,5,7-triphenyl-1H-1,3,2λ5,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ5-triazaphosphol)-10-yl>methylhydrazon-5'-oxid (86213-85-6,86286-46-6,344913-13-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / Et₃N / benzene

2: 68 percent / Et₃N / benzene / 1 h

3: CHCl₃

With triethylamine; In chloroform; benzene;

upstream raw materials:

N-Amino-9,10-dihydro-N,1,9-trimethyl-3,5,7-triphenyl-1H-1,3,2λ⁵,4-diazadiphospheto<2,1-c:2,3-c'>bis(1,2,4,3λ⁵-triazaphosphol)-10-amin-5-oxid

acetone

5,5,10,10-tetrachloro-1,6-dimethyl-3,8-diphenyl-1,5,6,10-tetrahydro-5λ⁵,10λ⁵-[1,3,2,4]diazadiphospheto[2,1-c;4,3-c']bis[1,2,4,3]triazaphosphole

P,P-dichlorophenylphosphine oxide

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