2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-

Base Information

Chemical Name:2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-
CAS No.:117585-58-7
Molecular Formula:C12H11BrN2
Molecular Weight:263.137
Hs Code.:
DSSTox Substance ID:DTXSID90472474
Nikkaji Number:J1.005.358G
Wikidata:Q82301438
Mol file:117585-58-7.mol

Synonyms:117585-58-7;2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-;2-[5-(bromomethyl)pyridin-2-yl]-5-methylpyridine;5-(Bromomethyl)-5'-methyl-2,2'-bipyridine;2-(5-(bromomethyl)pyridin-2-yl)-5-methylpyridine;5-bromomethyl-5'-methyl-2,2'-bipyridinyl;SCHEMBL8526622;DTXSID90472474

Suppliers and Price of 2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-

Chemical Property:

PSA：25.78000
LogP:3.34690
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:262.01056
Heavy Atom Count:15
Complexity:198

Purity/Quality:: 99.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CN=C(C=C1)C2=NC=C(C=C2)CBr

Technology Process of 2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl-

There total 5 articles about 2,2'-Bipyridine, 5-(bromomethyl)-5'-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 218304-01-9
5-(trimethylsilyl)methyl-5'-methyl-2,2'-bipyridine

: 117585-58-7
5-bromomethyl-5'-methyl-2,2'-bipyridine

Guidance literature:: With C₂Br₂F₄; cesium fluoride; In N,N-dimethyl-formamide; at 25 ℃; for 2h;
DOI:10.1016/S0040-4039(98)02041-3

Reference yield: 70.0%

: 1762-34-1
5,5'-dimethyl-2,2'-bipyridine

: 117585-58-7
5-bromomethyl-5'-methyl-2,2'-bipyridine

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 77 ℃; for 17h;
DOI:10.1021/ja054347j

Reference yield: 53.0%

: 1762-34-1
5,5'-dimethyl-2,2'-bipyridine

: 117585-58-7
5-bromomethyl-5'-methyl-2,2'-bipyridine

: 92642-09-6
5,5'-bis(bromomethyl)-2,2'-bipyridine

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 77 ℃; for 17h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1021/ic301810y