1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

Base Information

Chemical Name:1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine
CAS No.:75872-07-0
Molecular Formula:C₂₀H₂₁O₃P
Molecular Weight:340.359
Hs Code.:

1,1,4-trimethoxy-2,6-diphenyl-λ<sup>5</sup>-phosphorine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

Chemical Property:

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Technology Process of 1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

There total 5 articles about 1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54182-55-7
4-acetylamino-1,1-dimethoxy-2,6-diphenyl-λ⁵-phosphorine

: 75872-07-0
1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / conc. H₂SO₄ / ethanol / 2 h / Heating; further reagent: conc. HCl

2: K / hexamethylphosphoric acid triamide / 0.5 h

With sulfuric acid; potassium; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;

Reference yield:

: 54182-52-4
1,1-Dimethoxy-2,6-diphenyl-4-phenylazo-λ⁵-phosphorin

: 75872-07-0
1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Zn / acetic acid / 1 h / Ambient temperature

2: 51 percent / conc. H₂SO₄ / ethanol / 2 h / Heating; further reagent: conc. HCl

3: K / hexamethylphosphoric acid triamide / 0.5 h

With sulfuric acid; potassium; zinc; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; acetic acid;

Reference yield:

: 75872-06-9
1-Methoxy-2,6-diphenyl-1λ⁵-phospha-2-cyclohexen-1,4-dion

: 75872-07-0
1,1,4-trimethoxy-2,6-diphenyl-λ⁵-phosphorine

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / SeO₂ / butan-1-ol / 8 h / Heating

2: K / hexamethylphosphoric acid triamide / 0.5 h

With selenium(IV) oxide; potassium; In N,N,N,N,N,N-hexamethylphosphoric triamide; butan-1-ol;