Technology Process of C20H22N2O7
There total 12 articles about C20H22N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / 1,4-dioxane; water
2: 18-crown-6 ether / 1,4-dioxane
With
18-crown-6 ether; sodium hydroxide;
In
1,4-dioxane; water;
DOI:10.1016/j.bmcl.2011.06.104
- Guidance literature:
-
Multi-step reaction with 4 steps
1: oxalyl dichloride; dimethyl sulfoxide; triethylamine
2: sodium tetrahydroborate / methanol
3: sodium hydroxide / 1,4-dioxane; water
4: 18-crown-6 ether / 1,4-dioxane
With
sodium tetrahydroborate; oxalyl dichloride; 18-crown-6 ether; dimethyl sulfoxide; triethylamine; sodium hydroxide;
In
1,4-dioxane; methanol; water;
1: Swern oxidation;
DOI:10.1016/j.bmcl.2011.06.104
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sodium periodate
2: sodium hydroxide
4: sulfuric acid; acetic acid
5: trimethylsilyl trifluoromethanesulfonate; BSA
6: methanol; ammonia
7: oxalyl dichloride; dimethyl sulfoxide; triethylamine
8: sodium tetrahydroborate / methanol
9: sodium hydroxide / 1,4-dioxane; water
10: 18-crown-6 ether / 1,4-dioxane
With
methanol; sodium tetrahydroborate; sodium periodate; oxalyl dichloride; 18-crown-6 ether; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; BSA;
In
1,4-dioxane; methanol; water;
5: Vorbruggen reaction / 7: Swern oxidation;
DOI:10.1016/j.bmcl.2011.06.104
