Technology Process of C16H16N2O6S*C12H23N
There total 1 articles about C16H16N2O6S*C12H23N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium hydrogensulfate / ethyl acetate
2.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
2.2: 3 h / 0 - 20 °C / pH 7 - 8
3.1: acetic acid; zinc / 5 h / 20 °C
4.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
4.2: 0 - 20 °C / pH 8
5.1: sodium hydroxide / ethanol / 2 h / 20 °C
6.1: ethanol
7.1: 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / -15 °C
8.1: 4-methyl-morpholine / N,N-dimethyl-formamide / -15 - 20 °C
With
4-methyl-morpholine; potassium hydrogensulfate; acetic acid; sodium hydroxide; zinc;
In
ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm3012917
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: potassium hydrogensulfate / ethyl acetate
2.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
2.2: 3 h / 0 - 20 °C / pH 7 - 8
3.1: acetic acid; zinc / 5 h / 20 °C
4.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice
4.2: 0 - 20 °C / pH 8
5.1: sodium hydroxide / ethanol / 2 h / 20 °C
6.1: ethanol
7.1: 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / -15 °C
8.1: 4-methyl-morpholine / N,N-dimethyl-formamide / -15 - 20 °C
9.1: C18 column / acetonitrile; water
With
4-methyl-morpholine; potassium hydrogensulfate; acetic acid; sodium hydroxide; zinc;
In
ethanol; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm3012917
